مجال التميز | تميز دراسي وبحثي |
البحوث المنشورة |
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البحث (1): | |
عنوان البحث: |
Efficient Flow Electrochemical Alkoxylation of Pyrrolidine-1-carbaldehyde |
رابط إلى البحث: |
https://www.thiemeconnect.com/products/ejournals/abstract/10.1055/s-0037-1611774 |
تاريخ النشر: |
29/03/2019 |
موجز عن البحث: |
We report on the optimization of the alkoxylation of pyrrolidine-1-carbaldehyde by using a new electrochemical microreactor. Precise control of the reaction conditions permits the synthesis of either mono- or dialkoxylated reaction products in high yields. |
البحث (2): | |
عنوان البحث: |
Automated Electrochemical Selenenylations |
رابط إلى البحث: |
https://www.thiemeconnect.com/products/ejournals/abstract/10.1055/s-0039-1690868 |
تاريخ النشر: |
31/03/2020 |
موجز عن البحث: |
Integrated electrochemical reactors in automated flow systems were utilised for selenenylation reactions. The automation allowed multiple electrochemical reactions of a programmed sequence to be performed in a fully autonomous way. Many functionalised selenenylated products were synthesised in short reaction times in good to high yields. |
البحث (3): | |
عنوان البحث: |
Accelerating Electrochemical Synthesis through Automated Flow: Efficient Synthesis of Chalcogenophosphites |
رابط إلى البحث: | |
تاريخ النشر: |
16/06/2020 |
موجز عن البحث: |
Integrated electrochemical reactors in automated flow systems have been utilised for chalcogenophosphite formations. Multiple electrochemical reactions can be performed using a programmed sequence in a fully autonomous way. Differently functionalised chalcogenophosphites have been efficiently synthesised in short reaction times. |
المؤتمرات العلمية |
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المؤتمر (1): |
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عنوان المؤتمر: |
Flow chemistry Europe 2020 |
تاريخ الإنعقاد: |
03/03/2020 |
مكان الإنعقاد: |
Cambridge, UK |
طبيعة المشاركة: |
Poster presentation |
عنوان المشاركة: |
Automated Electrochemical Selenenylations |
ملخص المشاركة: |
Among emerging technologies to synthesize organic molecules, electrochemical reactors integrated in flow systems is one of the promising approaches to conduct electrochemical reactions. In this work we present an integrated electrochemical microreactor in flow using an automated Vapourtec device (R4-Series flow chemistry system) which we have utilized for selenenylation reactions. The automation has the potential to perform various electrochemical reactions in sequence with remote control. The equipment allows an automated synthesis of many derivatives in a short time. Involving this technique, various alkoxy and aza-selenenylation products have been synthesized including intramolecular reactions for the synthesis of heterocyclic compounds with good to high yields. |
ناصر جابر هادي عامري
دكتوراه
العلوم والتقنية
Cardiff University